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The synthesis of 13c-bilirubin and its use in the validation of bilirubin kinetic studies in rats
The total synthesis of [ 10-13C] bilirubin IXcx., the principal waste product of haem degradation, is described. Site specific labelling was accomplished by the Vilsmeier formylation of one of the dipyrrolic fragments using [1-13C] dimethylformamide. The penultimate dehydrohalogenation reaction was
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