HAL (France)
open access
Unexpected Oxidation of Co Nanoparticles Under H 2 : X‐Ray‐Induced Water Radiolysis in NAP‐XPS Studies
ABSTRACT Cobalt nanoparticles exposed to 1 mbar H 2 during near‐ambient‐pressure x‐ray photoelectron spectroscopy oxidize instead of reducing, a result that contradicts thermodynamic expectations. Using beam‐free references, flux‐dependent operando measurements, depth‐resolved spectra, and thermal c
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