HAL (France)
open access
(Hemi)synthesis of ribazole-2′,3′-cyclophosphate: a key building block in cobamide chemistry
This study presents a quick and effective method for producing α-ribazole-2',3'-cyclophosphate from vitamin B 12 . Using an optimized microwave-assisted cyanolysis, α-ribazole-2',3'-cyclophosphate was obtained in a high isolated yield of 90% after purification by silica column chromatography. This m
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